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src="http://ujianfei.com/static/picture/nindex2_1.jpg" >??? 行業(yè)新聞 </div> <div id="jjdx55f" class="nindexR1R"> 當前位置： <a href='http://.hk115-65.lfw.cn.comhttp://ujianfei.com'>主頁(yè)</a> > <a href='/style/hyzx/'>環(huán)亞資訊</a> > <a href='/style/hyxw/'>行業(yè)新聞</a> > 重點(diǎn)行業(yè)VOCs治理詳解之石化行業(yè) </div> </div> <div id="bpfz5lt" class="ninfoto">  <link rel="stylesheet" type="text/css" href="http://ujianfei.com/static/css/jquery.jqzoom.css" /> <script type="text/javascript" src="http://ujianfei.com/static/js/jquery.jqzoom-core.js"></script> <script type="text/javascript"> $(document).ready(function() { $('.jqzoom').jqzoom({ zoomType: 'standard', lens:true, preloadImages: false, alwaysOn:false, zoomWidth: 320, zoomHeight: 250 }); }); </script> <div id="hldzhnv" class="product_detail" id="pd1"> <h6 style="text-align: center;"><strong>? <span style="font-size: 24px;color: #333">重點(diǎn)行業(yè)VOCs治理詳解之石化行業(yè)</span></strong> <p class="smal-hide"><span>發(fā)布時(shí)間：2020-09-15 10:48</span> <span>點(diǎn)擊：<script src="/hyhb/count.php?view=yes&aid=2102&mid=1" type='text/javascript' language="javascript"></script></span></p> </h6> <div id="zzddvp7" class="wznr"><div> 揮發(fā)性有機物（VOCs）是形成 O3 及 PM2.5 的重要前體物。加強VOCs 治理是控制O3 和 PM2.5 污染的有效途徑，也是幫助企業(yè)實(shí)現節約資源、提高效益、減少安全隱患的有力手段。今天環(huán)亞環(huán)保結合國家發(fā)布的揮發(fā)性有機物治理手冊跟大家一起來(lái)學(xué)習下關(guān)于石化行業(yè)的VOCs廢氣治理，希望大家都能對于各類(lèi)重點(diǎn)行業(yè)的VOCs都能有一個(gè)詳細的了解，閉門(mén)造車(chē)終究難敵集思廣益，小編在看到文章的時(shí)候也是眼前一亮感覺(jué)受益匪淺，今天分享給大家。</div> <div> 石化行業(yè)生產(chǎn)裝置與 VOCs 排放環(huán)節示意見(jiàn)圖 1-1。石油煉制典型工藝流程及主要涉 VOCs 工藝有組織源項見(jiàn)圖 1-2。</div> <div> 石油化學(xué)典型工藝流程及主要涉 VOCs 工藝有組織源項見(jiàn)圖 1-3。<br /> <img alt="" src="/uploads/allimg/200915/1-20091510501Yc.png" style="width: 750px; height: 893px;" /><br /> <img alt="" src="/uploads/allimg/200915/1-20091510510H48.png" style="width: 750px; height: 513px;" /></div> <div> 那么我們該如何治理VOCs呢</div> <div> 首先從源頭削減</div> <div> （1）生產(chǎn)工藝</div> <div> ·宜采用全密閉、連續化、自動(dòng)化等生產(chǎn)技術(shù)。</div> <div> （2）裝置</div> <div> ·采樣口應采用密閉采樣或等效設施。</div> <div> ·企業(yè)內污染嚴重、服役時(shí)間長(cháng)的生產(chǎn)裝置和管道系統實(shí)施升級改造。</div> <div> ·宜選用無(wú)泄漏或泄漏量小的機泵和管閥件等設備。</div> <div> （3）輸送</div> <div> ·優(yōu)選采用管道輸送，減少罐車(chē)和油船裝卸作業(yè)及中間罐區。</div> <div> ·相近儲罐之間收發(fā)揮發(fā)性有機液體，可采用氣相平衡技術(shù)。</div> <div> · 含溶解性油氣物料（例如酸性水、粗汽油、粗柴油等），在長(cháng)距離、高壓輸送進(jìn)入常壓罐前，宜經(jīng)過(guò)脫氣罐回收釋放氣，避免閃蒸損失。</div> <div> （4）延遲焦化</div> <div> ·采用冷焦水密閉循環(huán)、焦炭塔吹掃氣密閉回收等技術(shù)。</div> <div> ·宜采用密閉除焦技術(shù)改造。</div> <div> （5）脫水脫氣</div> <div> ·采用密閉脫水、脫氣、摻混等工藝。</div> <div> （6）防腐防水涂裝</div> <div> ·采用低 VOCs 含量涂料替代溶劑型涂料。</div> <div> （7）污水處理場(chǎng)</div> <div> ·含油污水應密閉輸送，安裝水封等控制措施。</div> <div> ·盡可能減少集水井、隔油池數量，將污水溝渠管道化。</div> <div> ·集水井或無(wú)移動(dòng)部件隔油池可安裝浮動(dòng)蓋板（浮盤(pán)）。</div> <div> （8）循環(huán)水冷卻塔</div> <div> ·宜采用密閉式循環(huán)水冷卻系統。</div> <div> 然后過(guò)程控制</div> <div> （1）開(kāi)展設備與管線(xiàn)組件泄漏檢測與修復 (LDAR) 工作</div> <div> · 企業(yè)應識別載有氣態(tài) VOCs 物料、液態(tài) VOCs 物料的設備和管線(xiàn)組件的密封點(diǎn)，建立企業(yè)密封點(diǎn)檔案和泄漏檢測與修復計劃。</div> <div> · 宜建立企業(yè)密封點(diǎn)LDAR 信息平臺，全面分析泄漏點(diǎn)信息，對易泄漏環(huán)節制定針對性改進(jìn)措施。</div> <div> · 泵、壓縮機、閥門(mén)、開(kāi)口閥或開(kāi)口管線(xiàn)、氣體/ 蒸氣泄壓設備、取樣連接系統每三個(gè)月檢測一次。法蘭及其他連接件、其他密封設備每六個(gè)月檢測一次。</div> <div> （2）儲罐</div> <div> ·依據儲存物料的真實(shí)蒸氣壓選擇適宜的儲罐罐型。</div> <div> ·罐體應保持完好，不應有漏洞、縫隙或破損。</div> <div> · 固定頂罐附件開(kāi)口（孔）除采樣、計量、例行檢查、維護和其他正?；顒?dòng)外，應密閉；應定期檢查呼吸閥的定壓是否符合設定要求。</div> <div> · 浮頂罐浮頂邊緣密封不應有破損，支柱、導向裝置等附件穿過(guò)浮盤(pán)時(shí)，應采取密封措施。應定期檢查邊緣呼吸閥定壓是否符合設定要求。</div> <div> · 內浮頂罐浮盤(pán)與罐壁之間應采用液體鑲嵌式、機械式鞋形、雙封式等高效密封方式。</div> <div> · 外浮頂罐浮盤(pán)與罐壁之間應采用雙封式密封，且初級密封采用液體鑲嵌式、機械式鞋形等高效密封方式。</div> <div> ·<span style="white-space:pre"> </span>加強人孔、清掃孔、量油孔、浮盤(pán)支腿、邊緣密封、泡沫發(fā)生器等部件密封性管理，強化儲罐罐體及廢氣收集管線(xiàn)的動(dòng)靜密封點(diǎn)檢測與修復。</div> <div> ·宜采用油品在線(xiàn)調和技術(shù)。</div> <div> ·宜采取平衡控制進(jìn)出罐流量、減少罐內氣相空間等措施。</div> <div> ·常見(jiàn)石油煉制儲罐介質(zhì)、罐型、儲存溫度見(jiàn)表 1-1。<br /> <img alt="" src="/uploads/allimg/200915/1-20091510514A43.png" style="width: 750px; height: 632px;" /><br /> <img alt="" src="/uploads/allimg/200915/1-200915105156113.png" style="width: 750px; height: 532px;" /><br /> <img alt="" src="/uploads/allimg/200915/1-20091510520L14.png" style="width: 750px; height: 525px;" /><br /> <img alt="" src="/uploads/allimg/200915/1-20091510521B30.png" /><br /> <img alt="" src="/uploads/allimg/200915/1-200915105226159.png" style="width: 750px; height: 225px;" /><br /> <img alt="" src="/uploads/allimg/200915/1-2009151052362K.png" style="width: 750px; height: 184px;" /></div> <div> （3）裝卸</div> <div> ·宜采用快速干式接頭。</div> <div> · 嚴禁噴濺式裝載，采用頂部浸沒(méi)式裝載或底部裝載。頂部浸沒(méi)式裝載出油口距離罐底高度應小于 200 毫米。</div> <div> ·應密閉裝油并將油氣收集、輸送至回收處理裝置。</div> <div> 噴濺式裝載、頂部浸沒(méi)式裝載、底部裝載見(jiàn)圖 1-4 ～圖 1-6。<br /> <img alt="" src="/uploads/allimg/200915/1-200915105249148.png" style="width: 750px; height: 481px;" /><br /> <img alt="" src="/uploads/allimg/200915/1-200915105313493.png" style="width: 750px; height: 358px;" /></div> <div> （4）催化重整</div> <div> ·優(yōu)化調整催化劑再生溫度、供風(fēng)量等。</div> <div> （5）污水集輸與處理</div> <div> ·集水井（池）、調節池、隔油池、氣浮池、曝氣池、濃縮池等污水處理池應采用密閉收集措施，密閉材料應具有防腐性能，密閉蓋板應接近液面，負壓收集，回收或處理。</div> <div> ·優(yōu)化氣浮池運行，嚴格控制氣浮池出水中的浮油含量。</div> <div> （6）循環(huán)水冷卻塔</div> <div> · 對于開(kāi)式循環(huán)水，每六個(gè)月至少開(kāi)展一次循環(huán)水塔和含 VOCs 物料換熱設備進(jìn)出口總有機碳（TOC）或可吹掃有機碳（POC）監測工作，出口濃度大于進(jìn)口濃度 10% 的，要溯源泄漏點(diǎn)并及時(shí)修復。</div> <div> （7）火炬</div> <div> · 在任何時(shí)候，揮發(fā)性有機物和惡臭物質(zhì)進(jìn)入火炬都應能點(diǎn)燃并充分燃燒。</div> <div> ·禁止熄滅火炬系統長(cháng)明燈。</div> <div> ·設置視頻監控裝置。</div> <div> （8）非正常工況</div> <div> · 制定開(kāi)停車(chē)、檢維修、生產(chǎn)異常等非正常工況的操作規程和污染控制措施。</div> <div> ·裝置檢維修過(guò)程管理宜數字化，計量吹掃氣量、溫度、壓力等參數；宜通過(guò)輔助管道和設備等建立蒸罐、清洗、吹掃產(chǎn)物密閉排放管網(wǎng)。選用適宜的清洗和吹掃介質(zhì)。檢修過(guò)程產(chǎn)生的物料分類(lèi)進(jìn)入瓦斯管網(wǎng)和火炬系統，以及帶有廢氣處理裝置的污油罐、酸性水罐和污水處理場(chǎng)。</div> <div> · 做好檢維修記錄，并及時(shí)向社會(huì )公開(kāi)非正常工況相關(guān)環(huán)境信息，接受社會(huì )監督。</div> <div> · 非計劃性操作應嚴格控制污染，杜絕事故性排放，事后及時(shí)評估并向生態(tài)環(huán)境主管部門(mén)報告。</div> <div> 3.末端治理</div> <div> （1）儲罐</div> <div> · 儲存真實(shí)蒸氣壓≥ 5.2 kPa 但＜ 27.6 kPa 的設計容積≥ 150 m3 的揮發(fā)性有機液體儲罐，以及儲存真實(shí)蒸氣壓≥ 27.6 kPa 但＜ 76.6 kPa 的設計容積≥ 75 m3 的揮發(fā)性有機液體儲罐，若采用固定頂罐，應安裝密閉排氣系統至有機廢氣回收或處理裝置。</div> <div> · 采用吸收、吸附、冷凝、膜分離等 A 類(lèi)回收組合技術(shù)以及與蓄熱式燃燒、蓄熱式催化燃燒、催化燃燒等 B 類(lèi)破壞技術(shù)的組合技術(shù)，如 A+A，</div> <div> A+A+A，A+B，A+A+B 等。</div> <div> （2）裝卸</div> <div> ·<span style="white-space:pre"> </span>可采用吸收、吸附、冷凝、膜分離等 A 類(lèi)回收組合技術(shù)以及與蓄熱式燃燒、蓄熱式催化燃燒、催化燃燒等 B 類(lèi)破壞技術(shù)的組合技術(shù)，如</div> <div> A+A，A+A+A，A+B，A+A+B 等。</div> <div> · 甲醇、乙醇、環(huán)氧丙烷等易溶于水的化學(xué)品裝載作業(yè)排氣，宜采用水吸收或吸收 + 催化燃燒處理。</div> <div> （3）廢水液面</div> <div> · 隔油池、氣浮池等高濃度廢氣宜采用催化燃燒、焚燒等處理技術(shù)，不應采用低溫等離子、UV 光解等單一低效處理技術(shù)。</div> <div> ·曝氣池等低濃度廢氣可采用生物法、吸附、焚燒等處理技術(shù)。</div> <div> （4）工藝有組織</div> <div> · 重整催化劑再生煙氣、離子液法烷基化裝置催化劑再生煙氣脫氯后可采用焚燒、催化燃燒等處理技術(shù)。</div> <div> · 氧化脫硫醇尾氣可進(jìn)克勞斯尾氣焚燒爐處理，或采用低溫柴油吸收等處理技術(shù)。</div> <div> ·氧化瀝青尾氣宜采用焚燒等處理技術(shù)。</div> <div> · 乙二醇 / 環(huán)氧乙烷裝置乙二醇 / 環(huán)氧乙烷反應系統循環(huán)氣進(jìn)行焚燒處理。</div> <div> ·苯乙烯裝置多乙苯塔尾氣和真空泵密封罐尾氣作加熱爐燃料。</div> <div> · 聚苯乙烯裝置密封液罐尾氣宜通過(guò)控制冷凝溫度、設置除霧器回收液滴等措施降低不凝氣污染物濃度。</div> <div> · 苯酚丙酮裝置多異丙苯塔頂尾氣和氧化反應器尾氣應送至尾氣焚燒爐或催化燃燒處理，其他含有烴類(lèi)的廢氣應進(jìn)入火炬系統。</div> <div> ·聚乙烯、聚丙烯裝置尾氣宜采用催化燃燒、焚燒等技術(shù)。</div> <div> ·氯乙烯裝置工藝尾氣采用高溫焚燒處理，焚燒煙氣進(jìn)行吸收處理。</div> <div> ·精對苯二甲酸 PTA 生產(chǎn)尾氣宜采用高壓催化燃燒等處理技術(shù)。</div> <div> ·丙烯腈生產(chǎn)尾氣宜采用焚燒、催化燃燒等處理技術(shù)。</div> <div> · 橡膠生產(chǎn)尾氣宜采用預處理（冷凝、除霧、過(guò)濾、洗滌等）+ 催化燃燒、蓄熱式催化燃燒等處理技術(shù)。</div> <div> ·環(huán)氧丙烷 / 苯乙烯生產(chǎn)尾氣宜采用催化燃燒等處理技術(shù)。</div> <div> ·苯胺生產(chǎn)廢氣宜采用預處理（冷卻和除霧）+ 催化燃燒等處理技術(shù)。</div> <div> ·氯苯生產(chǎn)廢氣宜采用蓄熱燃燒 + 堿洗 + 吸附等處理技術(shù)。</div> <div> （5）固體廢物堆場(chǎng)</div> <div> · 廢催化劑、廢吸附劑、廢樹(shù)脂、蒸餾殘液等危險廢物貯存間廢氣應收集處理，可采用活性炭吸附等處理技術(shù)。</div> <div> （6）非正常工況</div> <div> · 裝置檢維修過(guò)程選用適宜的清洗劑和吹掃介質(zhì)；清掃氣應接入有機廢氣回收或處理裝置，可采用冷凝、吸附、吸收、催化燃燒等處理技術(shù)。</div> <div> · 在難以建立密閉蒸罐、清洗、吹掃產(chǎn)物密閉排放管網(wǎng)的情況下，采用移動(dòng)式設備處理檢修過(guò)程排放廢氣。</div> <div> · 生產(chǎn)設備在非正常工況下通過(guò)安全閥排出的含揮發(fā)性有機物廢氣應接入有機廢氣回收或處理裝置。</div> <div> 4.<span style="white-space:pre"> </span>排放限值</div> <div> · 車(chē)間或生產(chǎn)設施排氣筒排放的含 VOCs 廢氣和廠(chǎng)界 VOCs 無(wú)組織排放控制要求應符合《石油煉制工業(yè)污染物排放標準》（GB 31570—2015）、</div> <div> 《石油化學(xué)工業(yè)污染物排放標準》（GB 31571—2015）和《合成樹(shù)脂工業(yè)污染物排放標準》（GB 31572—2015）控制要求，有更嚴格地方標準的，執行地方標準。</div> <div> 5.<span style="white-space:pre"> </span>監測監控</div> <div> · 嚴格執行《排污許可證申請與核發(fā)技術(shù)規范<span style="white-space:pre"> </span>石化工業(yè)》（HJ 853—</div> <div> 2017）、《排污單位自行監測技術(shù)指南<span style="white-space:pre"> </span>石油煉制工業(yè)》（HJ 880—2017）和</div> <div> 《排污單位自行監測技術(shù)指南石油化學(xué)工業(yè)》（HJ 947—2018）規定的自行監測管理要求。</div> <div> ·納入重點(diǎn)排污單位名錄的石化企業(yè)，主要排污口安裝自動(dòng)監控設施，并與生態(tài)環(huán)境部門(mén)聯(lián)網(wǎng)。</div> <div> ·自動(dòng)監控等數據至少要保存一年，視頻監控數據至少保存三個(gè)月。</div> <div> · 鼓勵重點(diǎn)區域對無(wú)組織排放突出的企業(yè)，在主要排放工序安裝視頻監控設施。</div> <div> · 鼓勵企業(yè)配備便攜式 VOCs 檢測儀和紅外氣體成像儀（OGI），及時(shí)了解掌握排污狀況。</div> <div> · 具備條件的企業(yè)，通過(guò)分布式控制系統（DCS）等，自動(dòng)連續記錄環(huán)保設施運行及相關(guān)生產(chǎn)過(guò)程主要參數。DCS 監控等數據至少要保存一年。</div> <div> ·石化企業(yè) VOCs 監測指標及頻次要求見(jiàn)表 1-2。</div> <div> <img alt="" src="/uploads/allimg/200915/1-20091510534A40.png" style="width: 750px; height: 582px;" /></div> <div> 6.臺賬記錄</div> <div> 環(huán)境管理臺賬一般按日或按批次進(jìn)行記錄，異常情況應按次記錄。</div> <div> （1）生產(chǎn)基本信息</div> <div> · 生產(chǎn)裝置名稱(chēng)、主要工藝名稱(chēng)、生產(chǎn)設施名稱(chēng)、設施參數、原料名</div> <div> </div> <div> 稱(chēng)、產(chǎn)品名稱(chēng)、加工 / 生產(chǎn)能力、年運行時(shí)間、運行負荷以及原料、輔料、燃料使用量及產(chǎn)品產(chǎn)量等。</div> <div> （2）泄漏檢測與修復</div> <div> · 生產(chǎn)裝置名稱(chēng)、密封點(diǎn)類(lèi)型、密封點(diǎn)編號或位置、檢測時(shí)間、檢測初值、背景值、凈檢測值、介質(zhì)、檢測人等設備與管線(xiàn)組件密封點(diǎn)揮發(fā)性有機物泄漏檢測記錄表。</div> <div> ·是否修復、是否延遲修復、修復時(shí)間、修復手段、修復后檢測初值、修復后背景值、修復后凈檢測值、介質(zhì)、修復后檢測人等設備與管線(xiàn)組件密封點(diǎn)揮發(fā)性有機物泄漏修復記錄表。</div> <div> （3）儲罐</div> <div> · 罐型、公稱(chēng)容積、內徑、罐體高度、浮盤(pán)密封設施狀態(tài)、儲存物料名稱(chēng)、物料儲存溫度和年周轉量等以及儲罐維護、保養、檢查等運行管理情況、儲罐廢氣治理臺賬。</div> <div> （4）裝載</div> <div> · 裝載物料名稱(chēng)、設計年裝載量、裝載溫度、裝載形式（火車(chē)/ 汽車(chē) /</div> <div> 輪船 / 駁船）、實(shí)際裝載量等以及裝載廢氣治理臺賬。</div> <div> （5）火炬</div> <div> · 連續監測、記錄引燃設施和火炬的工作狀態(tài)（火炬氣流量、組成及熱值、火種氣流量）。</div> <div> （6）循環(huán)水冷卻系統</div> <div> · 服務(wù)裝置范圍、冷卻塔類(lèi)型、循環(huán)水流量、運行時(shí)間、冷卻水排放量、監測時(shí)間、監測濃度等。</div> <div> （7）廢水集輸、儲存與處理系統</div> <div> ·<span style="white-space:pre"> </span>廢水量、廢水集輸方式（密閉管道、溝渠）、廢水處理設施密閉情況、敞開(kāi)液面上方 VOCs 檢測濃度等。</div> <div> （8）治理設施運行信息</div> <div> · 按照設施類(lèi)別分別記錄設施的實(shí)際運行相關(guān)參數和維護記錄。具體參考第三部分中的“三、治理設施臺賬記錄”要求。</div> <div> （9）非正常工況</div> <div> · 生產(chǎn)裝置和污染治理設施非正常工況應記錄起止時(shí)間、污染物排放情況（排放濃度、排放量）、異常原因、應對措施、是否向地方生態(tài)環(huán)境主管部門(mén)報告、檢查人、檢查日期及處理班次等。</div> <div> </div> </div> <p id="cztz">版權聲明：本網(wǎng)注明來(lái)源為“環(huán)亞環(huán)?！钡奈淖?、圖片內容，版權均屬本站所有，如若轉載，請注明本文出處：http://ujianfei.com 。同時(shí)本網(wǎng)轉載內容僅為傳播資訊，不代表本網(wǎng)觀(guān)點(diǎn)。如涉及作品內容、版權和其它問(wèn)題，請與本網(wǎng)站聯(lián)系，我們將在及時(shí)刪除內容。</p> <p><br></p> <span id="v7jdj7b" class="czt"> <li id="tjyd"> 推薦閱讀：<a class="czt" href="/style/hyxw/2021/0524/2379.html">我國該如何實(shí)現碳中和？以下四條路徑或許是個(gè)辦法</a> </li> </span> <div id="7dlrlf7" class="page" 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